Abstract
Inelastic neutron scattering spectra (300–2500 cm −1) of KH(CHCO 2) 2, KD(CHCO 2) 2, KH(CDCO 2) 2 and KH(CHCO 2 · CClCO 2) have been obtained and the vibrations of the hydrogen bond, with the exception of ν 2(OHO), assigned. This is the first assignment of these vibrations in a centrosymmetric intramolecularly hydrogen bonded complex. ν as(OHO) was found to be heavily mixed and to give rise to a strong doublet in the INS spectra.
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