Abstract
This chapter deals with the high resolution NMR of solids. The chapter illustrates that with the development of multinuclear FT NMR spectrometers and the cross-polarization (CP) and magic angle sample spinning (MASS) techniques, there has been considerable recent interest in high-resolution NMR studies of solids. The chapter discusses several advantages of studying solids: Solid-state NMR provides an opportunity to study systems in the absence of intermolecular exchange (individual species). Moreover, solid-state NMR allows one to investigate the nature of the solid state and provides a bridge between X-ray data and solution NMR studies. With the increasing availability of commercial spectrometers designed specifically for solid-state work, and the practical and theoretical importance of many of the systems amenable to these techniques, this chapter concludes by expecting more activity in this area and a renewed interest in the solid state by chemists.
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