Abstract
Reversed-phase high-performance liquid chromatography was used to separate and isolate the glucuronic acid conjugate of 1,2,3-thiadiazole-5-carboxaldoxime from urine of rabbits after intravenous injection of the oxime. The conjugate was identified by gas chromatography—mass spectrometry as its trimethylsilylated methyl ester and by nuclear magnetic resonance spectrometry. Additional information was obtained from thin-layer chromatography and high-voltage paper electrophoresis.
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Schedule a callMore From: Journal of Chromatography B: Biomedical Sciences and Applications
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