Abstract
The theory of homonuclear decoupling combined with magic angle spinning is developed in the average Hamiltonian formalism. A description of pulse sequences used to tune for pulse width, pulse phase difference, and to minimize phase transient impurities is given. Resolution of n.m.r. spectra of 1 H in crystalline, partly crystalline and amorphous solids under various pulse sequences with and without magic angle spinning are illustrated. Sources of residual broadening are discussed.
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Schedule a callMore From: Philosophical Transactions of the Royal Society of London. Series A, Mathematical and Physical Sciences
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