Abstract

Hierarchically porous Fe3O4/C microspheres, with complex microstructures and excellent electrochemical performances as anode materials in LIBs, have been successfully prepared thanks to the self-aggregation of CO2 nano-bubbles confined by PVP and Fe(OH)3 nanoparticles decorated by citrate groups via the molecular chain entanglements during the condensation and carbonization of glucose.

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