Abstract

DOI: 10.1002/sscp.202200012 The cover picture represents the translation of repetitive reaction mixture analysis outside a fume hood using a conventional high performance liquid chromatography stack with manual syringe sampling to online analysis inside a fume hood using a simple, compact, hand-portable capillary liquid chromatograph that can be easily placed very close to the reaction vessel. The extremely small sample volume required for analysis by capillary liquid chromatography allows the use of miniature reaction vessels with minimal disturbance of the reaction mixture.

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