Abstract
The lamellar matrix VOPO4.2H2O was used to the intercalation of nitrosyl (NO) ligand. The vanadyl phosphate matrix, as well as the prepared intercalated compound (VOPO4.NO.H2O), were characterized by infrared spectroscopy, thermogravimetry, X-ray difractometry, and SEM microscopy. The X-ray diffraction patterns shown that the VOPO4.NO.H2O synthesis occurs with a decrease in the lamellar distance in comparison with VOPO4.2H2O. The SEM micrographs obtained for VOPO4.2H2O and VOPO4.NO.H2O shown that microstructure of vanadyl phosphate is flat square whereas the compound VOPO4.NO.H2O exhibits spheroid grains.
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