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Abstract
From conversions of Ar2SnH2 (Ar = Tripp, Dipp; Tripp = 2,4,6-Triisopropylphenyl, Dipp = 2,6-Diisopropylphenyl), and a bismuth(III) amide, Bi[N(SiMe3)2]3, we isolated the first representatives of mixed, uncharged Bi/Sn clusters, Bi8Sn3Ar6. Along with unprecedented bicyclo[2.2.0]hexanes, (HAr2Sn)2Sn2Bi4, these have been characterized by single crystal X-Ray diffraction, heteronuclear NMR, vibrational and UV-Vis spectroscopy. Quantum-chemical calculations were carried out in order to understand bonding within the isolated polyhedral compounds.
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