Abstract

A moire between crystal lattice planes and scanning electron beam-lines formed in a scanning transmission electron microscope includes the information of the lattice spacing. We apply these phenomena to a compositionally graded SiGe thin film deposited onto a Si substrate by molecular beam epitaxy method. The results of the experiments and image analysis show the potential of this technique to analyze a slight change of the lattice spacing according to a compositional change.

Highlights

  • A slight change of lattice spacing around hetero-interfaces of crystalline materials has an important role for their properties in most of the cases in general

  • The incidental beam condition of the scanning transmission electron microscopy (STEM) must be very stable in order to record the STEM moiré

  • It is clear in this figure that the scanning direction of the STEM, which is always horizontal in the STEM images, is almost parallel to the {111} plane of the specimen

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Summary

Introduction

A slight change of lattice spacing around hetero-interfaces of crystalline materials has an important role for their properties in most of the cases in general. In a field of semiconductor devices, lattice strains due to hetero-structures are important to realize high-speed transistors and we have been studying them [1] [2] [3] [4] [5]. Transmission electron microscopy (TEM) and scanning transmission electron microscopy (STEM) are useful to analyze this kind of local lattice spacing of crystals. TEM-based techniques such as high-resolution TEM/STEM images and nano-beam transmission electron diffraction techniques are not suitable for the wide range observation, for example, observation from the squared-micron order area. A very unique method to analyze lattice spacing has been reported by other researchers [6]-[12].

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