Abstract
Starting from a worrying observation, that companies have difficulties controlling the anomalies of their manufacturing processes, in order to have a better control over them, we have realized a case study on the practical data of the Fertial Complex to analyze the main parameters of the ammonia neutralization by nitric acid process. This article proposes a precise diagnostic of this process to detect dysfunction problems affecting the final product. We start with a general diagnosis of the process using the SPC method, this approach is considered an excellent way to monitor and improve the product quality and provides very useful observations that allowed us to detect the parameters that suffer from problems affecting the quality. After the discovery of the parameters incapable to produce the quality required by the standards, we applies two machine learning technologies dedicated to the type of data of these parameters for detected the anomaly, the first technique called The kernel connectivity-based outlier factor (COF) algorithm consists in recording for each object the degree of being an outlier, the second technique called the Isolation Forest, its principle is to establish a forest to facilitate the calculation and description. The results obtained were compared in order to choose which is the best algorithm to monitor and detect the problems of these parameters, we find that the COF method is more efficient than the isolation forest which leads us to rely on this technology in this kind of process in order to avoid passing a bad quality to the customer in future.
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