Abstract
A convenient preparation of both stereoisomers of a (2 R)/(2 S)-2- C-glycosylated β-amino acid is described. β- C-Glycoside was formed by the reaction of α-acetobromoglucose with carbanion of cyanoacetate. The steric bulk of the C-glycoside moiety does not hinder amino acid coupling, showing the utility of this carbohydrate-containing building block for glycopeptide synthesis.
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