Abstract

We developed a facile method to prepare CdIn 2S 4 monodispersed spherical particles by using mercaptoacetic acid as capping agent and thioacetamide as sulfur source. The results indicated that the size and morphology of CdIn 2S 4 particles were related to reaction time. The CdIn 2S 4 spherical particles with an average size of about 236 nm and a narrow size distribution were formed after reacting for 7 h. The photocatalytic activity of as-synthesized CdIn 2S 4 spherical particles was evaluated by the photocatalytic degradation of methyl orange under visible light illumination. The results showed that the photocatalytic activity increased with prolonging reaction time in the preparation of CdIn 2S 4 spherical particles. The CdIn 2S 4 spherical particles prepared after reacting for 7 h exhibited a 98% degradation efficiency of methyl orange after 15 min visible light irradiation.

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