Abstract
NiO prepared at 950° has been impregnated with a solution of copper nitrate and heated at 300°. The incorporation of CuO issued from this treatment in the lattice of NiO during sintering at 450–1100° has been studied by DTA and TG, and chemical analysis. A few experiments by radiocrystallographic analysis and electron diffraction have also been done. The process of incorporation begins at about 600° and is nearly complete at 900°. A sample elaborated at 1100° is homogeneous in the mass but presents in the surface an excess of copper ions which seems to be located at certain points.
Talk to us
Join us for a 30 min session where you can share your feedback and ask us any queries you have