Abstract
Single-crystal EPR spectra of the paramagnetic complex [Co 6 (μ 3 -S) 8 (PEt 3 ) 6 ] BPh 4 (PEt 3 =triethylphosphine; BPh 4 =tetraphenylborato anion) at 4.2 K were interpreted using a S=1/2 spin Hamiltonian with g x =2.35 (1), g y =2.04 (1), and g z =1.95 (1). The x, y, and z axes are close to the bond directions of one of the six inequivalent cobalt atoms. The compound is EPR silent at room temperature, both in the solid state and in solution
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