Abstract
Anodic oxidation of triphenylantimony in the presence of various oxygen nucleophiles or halide ions provided the corresponding hypervalent compounds having SbY bonds (Y = RCOO, F, Cl, Br) in good yields. On the contrary, anodic oxidation of triphenylbismuth gave only carbon-bismuth bond cleavage products. Cathodic reduction of anodically synthesized hypervalent organoantimony compounds was also investigated by cyclic voltammetry.
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