Abstract
The electrochemical reduction of aromatic and aliphatic sulfides has been investigated at Ag electrodes by means of surface-enhanced Raman spectroscopy (SERS) and cyclic voltammetry. The SERS technique applied to a rotating electrode system was demonstrated to be very useful for microscopic study of the electrochemical process on metal surfaces. We have proven the validity of the earlier proposition that addition of borohydride in aqueous Ag sol lowers the sol surface potential, enabling the electrochemical reduction of organic sulfides to thiolates
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