Abstract

Electrochemical intercalation–deintercalation of 18 M H 2SO 4 into graphite is examined in the acid solution free and admixed with 0.5 M MoO 3. The differences observed in the kinetics of reactions resulting from the presence of MoO 3 in H 2SO 4 allow an assumption that negatively charged molybdenum oxide and/or its intermediates are intercalated into graphite galleries together with sulphuric acid producing ternary H 2SO 4–MoO x –graphite intercalation compound (GIC).

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