Abstract

A detailed study on vertical electropolishing (VEP) of a 1.3-GHz single-cell niobium coupon cavity, which contains six coupons and four viewports at different positions, is reported. The cavity was vertically electropolished using a conventional rod and three types of unique cathodes named as Ninja cathodes, which were designed to have four retractable blades made of either an insulator or a metal or a combination of both. This study reveals the effect of the cathodes and their rotation speed on uniformity in removal thickness and surface morphology at different positions inside the cavity. Removal thickness was measured at several positions of the cavity using an ultrasonic thickness gauge and the surface features of the coupons were examined by an optical microscope and a surface profiler. The Ninja cathode with partial metallic blades was found to be effective not only in reducing asymmetric removal, which is one of the major problems in VEP and might be caused by the accumulation of hydrogen (${\mathrm{H}}_{2}$) gas bubbles on the top iris of the cavity, but also in yielding a smooth surface of the entire cavity. A higher rotation speed of the Ninja cathode prevents bubble accumulation on the upper iris, and might result in a viscous layer of similar thickness in the cavity cell. Moreover, a higher electric field at the equator owing to the proximity of partial metallic blades to the equator surface resulted in a smooth surface. The effects of ${\mathrm{H}}_{2}$ gas bubbles and stirring were also observed in lab EP experiments.

Highlights

  • A 1.3-GHz niobium (Nb) superconducting radiofrequency (SRF) cavity with a target field gradient of ∼35 MV=m and a high Q0 value of 1010 will be required for the future international linear collider (ILC) [1,2,3]

  • The rod cathode and Ninja cathodes (NC)-1 resulted in the asymmetric removal of Nb along the cavity length where the removal at the top iris was measured to be approximately 3 times higher than that at the bottom iris

  • The longitudinal asymmetric removal might be a result of the accumulation of H2 gas bubbles on the top iris surface since the bubble accumulation might reduce a viscous layer thickness to enhance the EP rate

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Summary

Introduction

A 1.3-GHz niobium (Nb) superconducting radiofrequency (SRF) cavity with a target field gradient of ∼35 MV=m and a high Q0 value of 1010 will be required for the future international linear collider (ILC) [1,2,3]. Electropolishing (EP), which is used to smoothen a surface by anodic dissolution in an electrolyte under mass transport control [7,8], was found to be a promising technique for the final surface treatment of Nb SRF cavities [9,10,11]. A Nb cavity, selected as an anode with aluminum (Al) as a counter electrode, is electropolished (EPed) in standard EP electrolyte (96 wt% H2SO4 and 48 wt% HF in a volumetric ratio of 9∶1) [12].

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