Effect of Trialkoxysilane/Aminosilane-Containing Universal Adhesive on Resin-Ceramic Microtensile bond strength and Ceramic Wettability: An In-vitro Study

Abstract

BackgroundThe dual-silane (trialkoxysilane/aminosilane) universal adhesive (UA) is claimed for its enhanced priming capacity of glass-ceramics. ObjectiveThis study evaluated the effect of organofunctional trialkoxysilane- and organofunctional trialkoxysilane/aminosilane-containing UAs on the long-term resin–ceramic microtensile bond strength (μTBS) and wettability of ceramic. MethodsHydrofluoric acid-etched lithium disilicate discs were distributed into four groups as follows: (control), no priming was performed; (MBN), primed using a silane-based primer (Monobond N); (SBU), primed using a trialkoxysilane-containing UA (Single Bond Universal Adhesive) and (SBP), primed using a trialkoxysilane/aminosilane-containing UA (Scotchbond Universal Plus Adhesive). Ceramic discs were cemented into blocks then sectioned into microbeams stored in distilled water at 37˚ for 1 year. The μTBS was evaluated followed by assessment of the failure modes. The contact angle of the two UAs was measured with a goniometer using the sessile drop technique. ResultsMBN significantly improved the resin-ceramic μTBS (31.71 ± 6.33 MPa) compared to the control group. The resin-ceramic μTBS obtained after priming using SBP (22.83 ± 3.42 MPa) was comparable to those of MBN. SBU showed significantly inferior resin-ceramic μTBS (16.02 ± 6.28 MPa) compared with MBN. Mixed failures mode patterns were the most frequent in the groups. The ceramic wettability of both UAs did not significantly differ. ConclusionCeramic priming using a UA with dual-silane monomers (organofunctional trialkoxysilane/aminosilane) resulted in long-term adhesion comparable to a silane-containing primer. Incorporating aminosilane monomer in UA formulation did not affect the wetting of characteristics of the UA solution and enhanced its glass-ceramic priming capacity. Clinical significanceThe use of UA with optimized silane content as a primer for glass-ceramics simplifies clinical adhesive procedures including resin cementation and repair of ceramic restorations.