Effect of solute Ni on thermal activation process of plastic deformation in Fe–18Cr single-crystal micropillars

Abstract

The aim of the present study was to identify the effect of solute Ni element on the plastic deformation and its thermal activation process of 18Cr ferritic stainless steels. Single-crystal micropillars with different diameters of approximately 2 and 5 μm were fabricated on the surface of Fe–18%Cr–Ni alloy sheets containing different contents of Ni (0–2 mass%). Compression tests were performed on the micropillars at different initial strain rates to investigate the strain rate sensitivity (m) of stress for the slip initiation and the specimen-size dependence of the m value. In micropillars with a small diameter of 2 μm, the Fe–18%Cr binary alloy specimen exhibited a relatively higher strain-rate sensitivity of initial slip stress (m = 0.12), whereas m was reduced to 0.01 by adding 2% Ni. The same trend was observed in micropillars with a larger size of approximately 5 μm. The experimental results were utilized to evaluate the activation volume of plastic deformation. The activation volumes of the Fe–18%Cr alloy and alloy containing 1% Ni followed the specimen-size dependence trend of activation volume in bcc metals; however, the alloy containing 2% Ni exhibited larger activation volumes, suggesting a different thermal activation process presumably due to the significant interaction that occurred between dislocations and solute Ni atoms in bcc solid-solutions.