Abstract

The piperazinyl thiocarbamide ((Z)-4-(2-(((1-methyl-1H-pyrrol-2-yl)methylene) amino) ethyl)-Nphenylpiperazine-1-carbothioamide) was synthesised by Fly-ash-:H3PO4 nano catalyst assisted ultrasonicated condensation of (N-(2-piperazin-1-yl) ethyl)-1-(1H-pyrrol-2-yl) methanimine and 1-isothiocyanato-4-methylbenzene in ethanol medium. In this condensation the obtained yield was more than 85%. The synthesized carbothioamide was characterized by their analytical and spectroscopic data. The effect of Fly-ash-:H3PO4 nano catalyst was investigated by obtained percentage of yield. Similarly, the effect of solvent also studied on this reaction.

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