Abstract
AbstractA multi‐functional flow set‐up was developed for the rate‐ and temperature‐controlled reduction of copper catalysts, their application in high‐pressure methanol synthesis and the determination of the copper surface area by N2O frontal chromatography. The influence of constant‐rate reduction on the catalytic properties of a ternary Cu/ZnO/Al2O3 catalyst was investigated. The temperature during the constant‐rate reduction was found to decrease, indicating autocatalytic kinetics, but no significant catalytic effect of the milder reduction conditions was observed compared with a slow linear heating ramp.
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