Abstract
Alumina–aluminium titanate (A–AT) composites are typically produced either by mixing the alumina matrix powder with already formed aluminium titanate or by reaction sintering of alumina and titania powders. Reaction-sintered materials usually exhibit limited final density and extensive microcracking. This paper describes the preparation of A–AT nanocomposites by slip casting and reaction sintering, using aqueous suspensions of submicrometre-sized alumina and nanometre-sized titania at a respective weight ratio of 87:13, which is typical for plasma-sprayed coatings. The colloidal stability of aqueous suspensions of the two individual powders and of their respective mixtures was determined first, measuring zeta potential and rheological behaviour as a function of deflocculant content and sonication time. The bimodal distribution yielded green relative densities of up to 70% of theoretical density. Dynamic and static sintering studies showed that aluminium titanate had already formed at 1400°C.
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