Directional coarsening of γ′ phase in single crystal nickel based superalloys during tensile creep

Abstract

The γ′ precipitate rafting kinetics and morphological evolution for two model single crystal superalloys have been studied. The microstructure of the alloys after different stages of tensile creep at 1040°C and under a range of stresses are examined using TEM and SEM. The chemical compositions of both γ and γ′ phases are analysed by energy dispersive spectrometry. Results show that a meshlike γ′ raft structure is formed along the direction normal to the stress axis during primary creep. The applied stress causes a decrease in the coherent strain energy at the γ′/γ interfaces in the (001) crystal plane. The released energy is the driving force for the diffusion of elements, leading to the formation of the γ′ rafts. A longer time is required for the formation of γ′rafts in alloy 2 owing to its higher content of the refractory element W which obstructs the migration of the other elements in the diffusion field of the γ′ rafts.