Abstract
Abstract A convenient electrochemical synthesis of various ML2, ML3, ML4 and MOL2 complexes (M = Ti, Zr,Hf, V,Cr, Mn,Fe, Co,Ni, Cu,In; L = acetylacetonate anion, 3-hydroxy-2-methyl-4-pyronate anion, 2-acetylpyrrolate anion, and other bidentate ligands) is described. The metal, as the anode of simple cell, is oxidised in the presence of the parent compound of the ligand (HL) in an organic solvent mixture. Gram quantities of complex can be produced in a few hours; other advantages of this method are discussed. Current efficiency measurements serve to identify the reaction mechanism.
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