Abstract
Trichloroacetylation of l-acyl-3-O-tert-butyldimethyl-silyl-sn-glycerols, followed by a direct conversion of the silyl protecting group into an ester functionality by means of a reagent system: tetra-n-butylammonium bromide (TBABr)-trimethylsilyl bromide (TMSBr)-carboxylic acid anhydride (CAA), constitutes an efficient protocol for the preparation of enantiomerically pure l,3-diacyl-sn-glycerols in high yields.
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