Abstract
A description is given of modifications which have been made to the remote cell used in conjunction with a DuPont 900 DTA such that the possibility of explosion is minimized. Using lead azide to evaluate the technique it is shown that complete curves for the exothermic decomposition ▪ are reproducibly obtained. The endotherm in the curve corresponding to the fusion of the product lead serves as a confirmation of the reaction. Illustrations are given to show extensions of the system to other sensitive compounds, namely lead styphnate, mercury fulminate, and potassium dinitrobenzfuroxan.
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