Development and evaluation of Moringa extract incorporated Chitosan/Guar gum/Poly (vinyl alcohol) active films for food packaging applications

Abstract

The present study contributes the synthesis of active films with the incorporation of moringa extract (ME) into chitosan (CS)/guar gum (GG)/poly(vinyl alcohol) (PVA) matrix (CGPM) by simple solvent casting technique. The effect of ME on the mechanical, thermal, structural and morphological properties of CGPM active films were investigated. ME has shown a marked influence on the optical, thermal properties and swelling behaviour of CGPM active films. The improvement in the tensile strength of CGPM-1 active film (53.7 MPa) was observed compared to control CS/GG/PVA (CGP) film. DSC study revealed that glass transition temperature (Tg) and melting temperature (Tm) decreased with the addition of ME in the CGP matrix, which confirmed the miscibility among the components of active films. There was an improvement in the thermal stability of the CGPM active films. The FTIR study confirmed the molecular interaction between ME and CS/GG/PVA matrix. The XRD analysis showed a decrease in crystallinity with an increase in the ratio of CS for CGPM active films. The CGPM active films were an excellent barrier to UV- light and have exhibited a decrease in moisture adsorption and water solubility compared to CGP control film. The inclusion of ME in the CGP matrix leads to the formation of a dense compact surface, which in turn enhanced hydrophobicity of active films. The CGPM active films showed minimum WVP, OP values and overall migration values were within the limits of 10 mg/dm2. It was also observed that CGPM active films effectively inhibited the growth of E. coli and S. aureus bacteria. These findings suggest CGPM active films are biodegradable, biocompatible, non-toxic and hence can find application as food packaging materials.