Deuterium permeation studies through bare and Er2O3 coated SS 316L

Abstract

Hydrogen isotope permeation through the structural walls of a fusion reactor poses concern for both fuel loss and safety. A primary focus in the International Thermonuclear Experimental Reactor (ITER) is the reduction of hydrogen isotopes, particularly tritium permeation through structural materials. In this work, an experimental setup has been developed to study the permeation of deuterium through thin samples such as bare and erbia (Er2O3) coated 100 µm thick stainless steel (SS 316 L). Permeation results through a bare SS 316 L sample yielded deuterium diffusivity and permeability of SS 316 L. Erbia coating on SS 316 L was developed using dip coating technique and its performance was tested as a permeation reduction barrier (PRB). A permeation reduction factor of ∼87 and 359 have been achieved with coating thickness ∼ 100 and ∼200 nm respectively. No measureable permeation flux was obtained for coating thickness of 492 nm. These results indicate the effectiveness of erbia coating in reducing deuterium permeation through SS 316 L.