Abstract

The determination of trace elements in metals by atomic absorption spectrophotometry with introduction of solid samples into furnaces has been reviewed from the first paper in 1965 until the present day. The need for this type of analysis is considered along with other analytical techniques that can provide useful information. Early developments up to 1975 are presented and discussed but the main emphasis is on work undertaken during the past five years. Information is provided on homogeneity of samples, methods of calibration, accuracy, precision and limits of detection to show that this technique is the most convenient available for the determination of volatile trace elements in metals at concentrations less than 10 μg g −1.

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