Abstract

One of the most common wastewater pollutants are organophosphorus pesticides, which have a complex of properties - high solubility, toxicity, mobility in the environment. In recent years, this method has become an innovative analytical technology for the most part used in medical practice and in pharmaceuticals. With development, the method begins to acquire a practical application in other branches of human life activity [1,2]. In this paper, the results of studies on the detection of Malathion (MLT)-O, O-Dimethyl-S- (1,2-dicarbethoxyethyl) dithiophosphate in aqueous media. The purpose of this study was to develop liquid chromatography & mass spectroscopy method for the determination of Malathion in water solution. This method will provide experimental results from testing conducted to evaluate sensitivity, selectivity, linearity, precision, accuracy, dilution integrity and various additional stability tests.

Highlights

  • Archives of Organic and Inorganic Chemical SciencesDetermination of Malathion in Water Using Liquid Chromatography & Mass Spectroscopy. Torosyan GH*, Armudjyan EK, and Davtyan VA National polytechnic university of Armenia, Yerevan Received: January 25, 2018; Published: February 05, 2018 *Corresponding author: Gagik Torosyan, National polytechnic university of Armenia, 37 Sayat-Nova str., apt. 10 Yerevan 375025, Yerevan, Armenia, Email: One of the most common wastewater pollutants are organophosphorus pesticides, which have a complex of properties - high solubility, toxicity, mobility in the environment

  • The Experiments were carried out using HPLC Grade Methanol, Acetonitrile and Deionized water supplied by Carl Roth, Germany

  • Serial dilution were made to obtain a final concentration of nine Calibration Curve Standards Working Solutions (CCS WS) as 1.0, 2.0, 5.0, 10.0 20.0 50.0, 100.0, 200.0 and 500.0ng/mL respectively

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Summary

Archives of Organic and Inorganic Chemical Sciences

Determination of Malathion in Water Using Liquid Chromatography & Mass Spectroscopy. Torosyan GH*, Armudjyan EK, and Davtyan VA National polytechnic university of Armenia, Yerevan Received: January 25, 2018; Published: February 05, 2018 *Corresponding author: Gagik Torosyan, National polytechnic university of Armenia, 37 Sayat-Nova str., apt. 10 Yerevan 375025, Yerevan, Armenia, Email: One of the most common wastewater pollutants are organophosphorus pesticides, which have a complex of properties - high solubility, toxicity, mobility in the environment. 10 Yerevan 375025, Yerevan, Armenia, Email: One of the most common wastewater pollutants are organophosphorus pesticides, which have a complex of properties - high solubility, toxicity, mobility in the environment In recent years, this method has become an innovative analytical technology for the most part used in medical practice and in pharmaceuticals. The purpose of this study was to develop liquid chromatography & mass spectroscopy method for the determination of Malathion in water solution. This method will provide experimental results from testing conducted to evaluate sensitivity, selectivity, linearity, precision, accuracy, dilution integrity and various additional stability tests

Reagents and Equipment
Conditions of Mass Spectrometry
Preparation of Standards Working Solutions
Sample Preparation
Method Performance Check Results
Arc Org Inorg Chem Sci
Conclusion
Full Text
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