Abstract

SummaryA robust method for analysing acrylamide in plantain and cassava snacks was developed using SPME and GC‐FID. Optimised via Box–Benkhen design, the method met European standards with a calibration curve R2 > 99%, detection limit 63 μg kg−1, and quantification limit 212 μg kg−1. Precision was <17.76% as per Horwitz equation. Acrylamide levels in fried ripe plantain were 894.40 ± 56.35 μg kg−1 and in cassava snacks 59.42 ± 2.46 μg kg−1. This validated method offers an efficient means for acrylamide control in thermally processed foods.

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