Densification of complex shape ceramics parts by SPS

Abstract

Spark Plasma Sintering (SPS) equipments, with higher productivity and hybrid heating modes, allow reducing thermal gradients in large samples and broaden their application potential. Furthermore, strong shape limitations remain: only simple shapes can be obtained because of the use of uniaxial pressure.The aim of this paper is to propose a SPS densification method for complex shape ceramic or powder metallurgy parts, without any modification of the tools and equipment. The samples to be sintered are placed in a powder bed in the classical die used in SPS. Different powder beds have been tested.A numerical model was developed in order to allow a rapid simulation of the force field around a part surrounded by a powder bed in a SPS tool. The optimization of the operating conditions was carried out, first, on small simple-shape samples, then, on complex geometry parts which were densified to demonstrate the feasibility of the proposed sintering process.