Abstract
Experiments have shown that certain mechanical properties can be greatly enhanced when a material is stressed while under tight spatial constraint. In this work, the post-yield behaviour of brittle and ductile epoxy resins used as thin adhesive bonds was determined using the “napkin ring” shear test. Real-time observations of the deformation in the bond as well as SEM post-failure analysis were employed to gain information on the failure process. The complete stress-strain histories of the adhesives were established for bond thicknesses ranging from the micrometre level up to values large enough to expose the bulk properties. The most dramatic variations occurred for the ultimate shear strain, γf; for the brittle adhesive, γf increased by over 30-fold relative to the bulk material when the bond thickness, t, was decreased to a few micrometres. Experimental evidence and analytical considerations suggest that the decline of γf with t was due to premature bond failure caused by tensile microcracks or voids that were formed in the interlayer during loading, with the specific γf versus t relationship being a mere reflection of the variations in the degree of stress concentration at the tip of the flaws. The astonishingly large value of γf (i.e. 2.8–3.4) found for the brittle epoxy in the micrometre thickness range, is believed to represent the intrinsic shear strain of this material.
Published Version
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