Abstract

Time-resolved X-ray tomographic microscopy is an invaluable technique to investigate dynamic processes in 3D for extended time periods. Because of the limited signal-to-noise ratio caused by the short exposure times and sparse angular sampling frequency, obtaining quantitative information through post-processing remains challenging and requires intensive manual labor. This severely limits the accessible experimental parameter space and so, prevents fully exploiting the capabilities of the dedicated time-resolved X-ray tomographic stations. Though automatic approaches, often exploiting iterative reconstruction methods, are currently being developed, the required computational costs typically remain high. Here, we propose a highly efficient reconstruction and classification pipeline (SIRT-FBP-MS-D-DIFF) that combines an algebraic filter approximation and machine learning to significantly reduce the computational time. The dynamic features are reconstructed by standard filtered back-projection with an algebraic filter to approximate iterative reconstruction quality in a computationally efficient manner. The raw reconstructions are post-processed with a trained convolutional neural network to extract the dynamic features from the low signal-to-noise ratio reconstructions in a fully automatic manner. The capabilities of the proposed pipeline are demonstrated on three different dynamic fuel cell datasets, one exploited for training and two for testing without network retraining. The proposed approach enables automatic processing of several hundreds of datasets in a single day on a single GPU node readily available at most institutions, so extending the possibilities in future dynamic X-ray tomographic investigations.

Highlights

  • Time-resolved X-ray tomographic microscopy is an invaluable technique to investigate dynamic processes in 3D for extended time periods

  • The simultaneous iterative reconstruction technique (SIRT)-filtered back-projection (FBP)-mixedscale dense convolutional network (MS-D)-DIFF classified water volumes of the three cells PEFC_1, PEFC_2 and PEFC_3 and the corresponding manual segmentations are presented in Figs. 3a, 4a and 5a, respectively

  • To allow comparison to the manual segmentations, the same masks were applied to all SIRT-FBPMS-D-DIFF reconstructions

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Summary

Introduction

Time-resolved X-ray tomographic microscopy is an invaluable technique to investigate dynamic processes in 3D for extended time periods. Because of the limited signal-to-noise ratio caused by the short exposure times and sparse angular sampling frequency, obtaining quantitative information through post-processing remains challenging and requires intensive manual labor. This severely limits the accessible experimental parameter space and so, prevents fully exploiting the capabilities of the dedicated time-resolved X-ray tomographic stations. To reach the required sub-second time resolution, both angular sampling frequency and exposure time are minimized leading to noisy datasets, which after tomographic reconstruction with standard analytical reconstruction algorithms result in low signal-to-noise ratio (SNR) volumes with undersampling ­artifacts[13]. The computational time remained still relatively high on limited computational resources

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