Abstract
Crystals of monoclinic Cu 2SnS 3 have been prepared by a conventional solid-state reaction. The crystal structure has been refined from a twinned specimen using X-ray diffraction data collected with an automatic diffractometer applying a high-dimensional twin refinement technique: space group Cc, a = 6.653(1), b = 11.537(2), c = 6.665(1) Å, β = 109.39(3)°, Z = 4, R F = 0.036, and wR F = 0.038 for 1237 reflections and 52 structural parameters. The structure is a superstructure of the sphalerite type structure, based on cubic close packing of S with order arrangement of Cu and Sn in tetrahedral sites, and it is isomorphic with Cu 2GeS 3 and Cu 2SiS 3.
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