Abstract
The variable temperature 1H, 13C and 31P NMR spectra of the complex [HRu3(CCBut)(CO)7(dppm)] (dppm Ph2PCH2PPh2), which crystallizes as an ordered racemic array of the two enantiomers, reveals a fluxional behaviour induced by the diphosphine, involving racemization via acetylide rotation and concurrent hydride migration.
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