Abstract
1. The corrected name of HCF2CF2CF2CF2OCF2CF2SO3 is ‘‘1,1,2,2tetrafluoro-2-(1,1,2,2,3,3,4,4-octafluorobutoxy)ethanesulfonate’’. Therefore, ‘‘1,1,2,2-tetrafluoro-2-(1,1,2,2-tetrafluoroethoxy)ethanesulfonate’’ in the article should be changed to ‘‘1,1,2,2tetrafluoro-2-(1,1,2,2,3,3,4,4-octafluorobutoxy)ethanesulfonate’’. 2. The missing parts for the synthesis of HCF2CF2CF2CF2OCF2CF2SO3Na and HCF2CF2CF2CF2OCF2CF2SO3H should be added to the experimental section as follows. To a stirred solution of 1,1,2,2-tetrafluoro-2-(1,1,2,2,3,3,4,4octafluorobutoxy)ethanesulfonyl fluoride (120 g, 0.3 mol) in ethanol (100 ml), the solution of sodium hydroxide (24 g, 0.6 mol) in water (100 ml) was added slowly at room temperature. Then the mixture was refluxed for 2 h. Removing the solvent under reduced pressure gave a solid. The solid was dissolved in ethyl acetate (200 ml) and the solutionwaswarmed
Published Version
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