Abstract
The study of grain-dependent corrosion behaviors of practical polycrystalline metals remains challenging due to the difficulty in eliminating the influences of other microstructural features, such as intermetallic particles and grain boundaries. In this work, we performed thousands of microscopic potentiodynamic polarization measurements on a polycrystalline alloys using the spatially resolved oil-immersed scanning electrochemical cell microscopy measurement. This work highlights the capability of oil-immersed scanning electrochemical cell microscopy in resolving small electrochemical differences, which will greatly promote the study of grain-dependent behaviors of practical polycrystalline samples.
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