Abstract

Membrane distillation (MD) is a relatively new and underdeveloped separation process which can be classified as a green technology. However, in order to investigate its dark points, sensitivity analysis and optimization studies are critical. In this work, a number of MD experiments were performed for concentrating glucose syrup using a sweeping gas membrane distillation (SGMD) process as a critical step in bioethanol production. The experimental design method was the Taguchi orthogonal array (an L9 orthogonal one) methodology. The experimental results showed the effects of various operating variables, including temperature (45, 55, and 65 °C), flow rate (200, 400, and 600 ml/min) and glucose concentration (10, 30, and 50 g/l) of the feed stream, as well as sweeping gas flow rate (4, 10, and 16 standard cubic feet per hour (SCFH)) on the permeate flux. The main effects of the operating variables were reported. An ANOVA analysis showed that the most and the least influenced variables were feed temperature and feed flow rate, each one with 62.1% and 6.1% contributions, respectively. The glucose rejection was measured at 99% for all experiments. Results indicated that the SGMD process could be considered as a versatile and clean process in the sugar concentration step of the bioethanol production.

Highlights

  • The increasing global energy demand and its ensuing crisis, as well as the highlighting of major environmental challenges in recent years have led to considerable interest for substituting hydrocarbon fuels with renewable and sustainable energy sources [1,2,3,4]

  • The Taguchi experimental design and optimization were investigated for the sensitivity analysis of concentrating the glucose syrups using the sweeping gas membrane distillation (SGMD) process

  • Feed temperature and sweeping gas flow rate showed the main effects on the permeate flux

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Summary

Introduction

The increasing global energy demand and its ensuing crisis, as well as the highlighting of major environmental challenges in recent years have led to considerable interest for substituting hydrocarbon fuels with renewable and sustainable energy sources [1,2,3,4]. Among the different renewable energies, biofuels, and in particular bioethanol as a clean fuel, have gained a great deal of attention [5,6,7]. Either in place of gasoline or in the form of an ethanol–gasoline, can reduce global warming emissions up to 80%. This can entirely eliminate the release of acid rain [8]. Bioethanol can be mixed with gasoline for transportation purposes. This technique has been widely used in several countries such as Brazil. Membrane processes have gained a great deal of attention for their various applications [9,10]

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