Abstract
Purpose of research: to obtain chitosan films with improved performance properties by using water activated by an electromagnetic field of the radio frequency range as a solvent. Objects of research: water activated by an electromagnetic field of the radio frequency range (90-200 MHz), as well as chitosan solutions and films obtained using it. Methods of research: conductometry, potentiometry, densitometry, viscometry, turbidimetry, gravimetry, IR spectroscopy are used in the work. To determine the deformation and strength characteristics of the films, a universal testing machine with an electromechanical drive УТС-110M was used. Main results of research: The effect of pretreatment of water with an electromagnetic field of various frequencies on the properties of acetic acid (2 %) chitosan solutions in the concentration range of 0.1-2.0% has been studied. A decrease in surface tension by 2.0–5.2 % was found, as well as an increase in light transmission by 10-30 % and viscosity of solutions by 24-37 % at a chitosan concentration of 1.0-2.0 %. These effects are most pronounced for frequencies of 70, 90, 110 and 130 MHz. Films were prepared from 2 % chitosan solutions and their deformation-strength and sorption characteristics with respect to water vapor were determined. The greatest increase in tensile strength was found for chitosan films obtained from solutions prepared on water activated by an electromagnetic field with frequencies of 70 and 110 MHz (38 and 23 %, respectively). A decrease in the hygroscopicity of films and an increase in the intensity of bands in the IR spectra of films obtained using activated water were found.
Published Version
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