Abstract
Direct separation of racemic tetrahedral transition metal carbonyl cluster SFeCoMo(CO)8(C2H5OCOCp) has been conducted by liquid chromatography using tribenzoylcellulose as chiral stationary phase. The effects of concentration of 2-propanol, various primary alcohols in the mobile phase and column temperature on the rentention and enantioselectivity of SFeCoMo(CO)8(C2H5OCOCp) cluster enantiomers were studied. The maximum resolution factor obtained was 2.306 when hexane/2-propanol(99.5/0.5,v/v) was used as solvent at 23°C.
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