ChemInform Abstract: The Unprecedented Tetrakis‐(disulfato)‐silicate Anion [Si(S2O7)4]4‐, Its Germanium Congener [Ge(S2O7)4]4‐, and the Tris‐(disulfato)‐metallates [M(S2O7)3]2‐ (M: Si, Ge, Ti), Stabilized by Divalent Counter Cations B2+ (B: Sr, Ba, Pb).

Christian Logemann,Mathias S Wickleder,Katja Riess

doi:10.1002/chin.201314020

ChemInform Abstract: The Unprecedented Tetrakis‐(disulfato)‐silicate Anion [Si(S2O7)4]4‐, Its Germanium Congener [Ge(S2O7)4]4‐, and the Tris‐(disulfato)‐metallates [M(S2O7)3]2‐ (M: Si, Ge, Ti), Stabilized by Divalent Counter Cations B2+ (B: Sr, Ba, Pb).

Christian Logemann, Mathias S Wickleder + Show 1 more

https://doi.org/10.1002/chin.201314020

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Journal: ChemInform

Publication Date: Mar 20, 2013

Affiliation: Carl von Ossietzky University of Oldenburg

#Sealed Glass Ampules #Reaction Of MCl4 + Show 4 more

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Abstract

AbstractThe compounds Sr2[M(S2O7)4] (M: Si, Ge), Ba[M(S2O7)3] (M: Si, Ge, Ti), and Pb[M(S2O7)3] (M: Ge, Ti) are prepared by reaction of MCl4 (M: Si, Ge, Ti) and BX (B: Sr, Ba, Pb; X: CO3, SO4) with oleum (sealed glass ampules, 100—250 °C, 12—14 h).

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