Abstract
Abstract(H2DABCO) [FeIII2F8(H2O)2] (I), (H2DABCO)2 [FeIII2F10]·2H2O (II), (HDABCO)4 [FeIII2F10]·10H2O (III), and (HFDABCO)[(FeII(H2O)6) (FeIIIF6)] (IV) are prepared by conventional solvothermal synthesis using a EtOH or DMF solution of FeF2, FeF3, and HF (4%) with DABCO (autoclave, 120 °C, 72 h) to explore the composition space diagram of the (Fe2+,Fe3+)‐DABCO‐HFaq chemical system.
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