Abstract

AbstractColorless crystals of [Mn(H2PO2)2]n·0.11DMF are solvothermally synthesized by reaction of MnCl2 with H3PO2 in a 8:1:1 (v/v) mixture of DMF, H2O, and EtOH (autoclave, 140 °C, 48 h, 60% yield).

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