Abstract
A chemical reaction for the preparation of B–C–N compounds by usingcarbon tetrachloride (CCl4), boron tribromide (BBr3),lithium nitride (Li3N) and sodium as reactants has been carriedout at the temperature of 400°C. Measurements of FTIR, XRD, TEM andEELS show that two kinds of compounds have been formed in the preparedsample. One is hollow sphere-like C–N with an amorphous structure; theother is piece-like polycrystalline B–C–N with the hexagonalstructure. Their determined compositions are close to C3N andBC2N, respectively.
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