Abstract
In the present chapter, we have reviewed the artificially engineered metal oxide nanomaterials using solvothermal methods, starting from the definition, historical development, instrumentation, and working as well as the key parameters affecting the nucleation and crystal growth of metal oxide nanomaterials. Subsequently, we have discussed the synthesis of some important unsupported metal oxide nanoparticles such as CeO2, CuO, ZrO2, ϒ-Fe2O3, TiO2, Cu2O, NiO, BaTiO3, and LiNbO3 and the effect of oxidants and solvents on the morphologies and size of metal oxide nanoparticles in the solvothermal methods with advantages and disadvantages.
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