Abstract
The detection and evaluation of mixed valence states in cation radical salts (CRS) of the tetrathiafulvalene (TTF) series are readily achieved by using thin layer cyclic voltammetry (TLCV) with an internal coulometric reference. The method has proved to be valid for the mixed valence determination of the following typical well known CRS : TTFBr0.75, TMTTF(PF6)0.5, TMTSF(PF6)0.5, BEDTTTF(PF6)0.5, BEDTTTF(BF4)0.5.
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