Abstract
Abstract Cd 3 [Cr(CN) 6 ] 2 · 14H 2 O crystallizes in a cubic unit cell, space group Fm3m(O h 5 , No. 225), with a 0 = 10.961(2)A. The observed density is 1.70(1) Mg-m −3 (calculated density, 1.690 Mg-m −3 ). A thermogravimetric analysis has yielded 13.9(2) water molecules per formula unit. X-Ray fluorescence emission energy values and infrared spectroscopic results are presented. Full-matrix least-squares refinement of 160 unique reflections has yielded R 1 = 0.0350 and R 2 = 0.0349. The disordered structure contains 1 1 3 molecules in the unit cell. Linkage of the divalent Cd atoms to the Cr atoms is accomplished by cyanide bridging. A new structural model was employed and important bond distances are reported.
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