Abstract
Bisarylamines with o-alkoxy substituents [o-NH2-C6H4-O(CH2)1/2/3]2 react with [nBu4N]4[α-Mo8O26] in anhydrous acetonitrile in the presence of N,N′-dicyclohexylcarbodiimide (DCC) to form a series of nanoscale molecular bola, bisorganoimido-bridged hexamolybdates with flexible alterable lengths, in which two hexamolybdate cages are connected by the bisarylimido linkers (see scheme).
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